Debye
Scherrer camera:
A very
small amount of powdered material is sealed into a fine capillary tube made from glass
that does not diffract x-rays. The specimen is placed in the Debye Scherrer
camera and is accurately aligned to be in the centre of the camera. X-rays enter the
camera through a collimator.
The powder diffracts the x-rays in accordance with Braggs law
to produce cones of diffracted beams. These cones intersect a strip of photographic film
located in the cylindrical camera to produce a characteristic set of arcs on the film.
Investigate the powder diffraction
method using the simulation here, by clicking on the start button repeatedly.
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Powder diffraction film:
When the film is removed from the
camera, flattened and processed, it shows the diffraction lines and the holes for the
incident and transmitted beams.
There are
always two arcs in the x-ray beams Ka and Kb, this causes the highest
angle back-reflected arcs to be doubled. From noting this, it is always clear which hole
is for the transmitted beam and which is for the incident beam in the film. |
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